14. Tom had been studying French hard for nearly three years     he mastered it.

A. after       B. when

C. since      D. before

14.   D考查狀語從句的連接詞。句意："湯姆努力學(xué)了將近三年后才精通了法語"。before意為"在……之前;……之后， 才……；沒來得及就……"。根據(jù)句意選D。

題目來源：2015全品語法快練高中英語新課標(biāo) > 訓(xùn)練4從句綜合訓(xùn)練

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